HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzyl chloride → HCID 19357861, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzyl chloride | HCID 7482 | — |
| Reactant | 5-(3,4-Dimethoxyphenyl)-3,6-dihydro-2H-1,3,4-thiadiazin-2-one | HCID 13365850 | — |
| Product | HCID 19357861 | HCID 19357861 | — |
Reaction Steps
In analogy to Example 1, the reaction of 5-(3,4-dimethoxyphenyl)-3,6-dihydro-1,3,4-thiadiazin-2-one ("B") with 4-nitrobenzyl chloride gives 3-(4-nitrobenzyl)-5-(3,4-dimethoxyphenyl)-3,6-dihydro-1,3,4-thiadiazin-2-one, m.p. 155°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06025354 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-5088e728f5394cb98f3f20b437d97245 |
| Source note | uspto-grants-2000_02 |