HCID 57086712, compound → HCID 57106440, compound

HRID 377322Notes

Reaction equation

HRID 377322 reaction equation
O[CH:2]([C@@H:11]1[CH2:16][CH2:15][CH2:14][CH2:13][C:12]1=[O:17])[C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([O:9][CH3:10])[CH:4]=1>C(O)C>[CH3:10][O:9][C:5]1[CH:4]=[C:3]([CH:8]=[CH:7][CH:6]=1)[CH2:2][C@@H:11]1[CH2:16][CH2:15][CH2:14][CH2:13][C:12]1=[O:17]

Participants

3

Reactant 1

HCID 57086712HCID 57086712, compound

Product 1

HCID 57106440HCID 57106440, compoundYield 107.3%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

To a solution of (2S)-2-[1-hydroxy-1-(3-methoxyphenyl)methyl]cyclohexanone (0.8 g) in ethanol (20 ml) was added paradium on carbon (0.5 g). After being stirred for 4 hours under hydrogen atmosphere, the reaction mixture was filtered. The solvent was evaporated to give (2S)-2-(3-methoxybenzyl)cyclohexanone (0.8 g).

Workup

  1. filtrationthe reaction mixture was filtered
  2. customThe solvent was evaporated

Sources & evidence

ORD record
ord-efab41b2cd164e8e881be282ac8bc9bd
Source dataset
uspto-grants-2000_02
Patent number
US06025375

Reaction notes

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