HuagongsheHuagongshe Chemistry Print Report · For research reference only
Perfluorooctyl iodide → 2-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoroundec-2-enyloxy)ethyl hydrogen sulfate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Perfluorooctyl iodide | HCID 10491 | — |
| Reactant | Allyloxyethyl sulfate | HCID 20611889 | — |
| Product | 2-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoroundec-2-enyloxy)ethyl hydrogen sulfate | HCID 131730836 | — |
Reaction Steps
Crystalline allyloxyethyl sulfate (Na salt) from the preparation shown in example 2 was perfluoroalkylated using the procedure of example 7 and C8F17I to produce 2-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundec-2-enyloxy)ethyl hydrogen sulfate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08524104B1 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-9ce66c0ac6a9497f90fd9e34b54bd9d0 |
| Source note | uspto-grants-2013_09 |