1-Methylimidazole → HCID 178464030, compound

HRID 377435Notes

Reaction equation

HRID 377435 reaction equation
[CH3:1][N:2]1[CH:6]=[CH:5][N:4]=[CH:3]1.[ClH:7].[CH2:8]([N:10]([CH2:14][CH3:15])[CH2:11][CH2:12][Cl:13])[CH3:9]>C(O)C>[ClH:13].[Cl-:7].[CH2:8]([N:10]([CH2:14][CH3:15])[CH2:11][CH2:12][N+:4]1[CH:5]=[CH:6][N:2]([CH3:1])[CH:3]=1)[CH3:9]

Participants

4

Reactant 2

HCID 13901-MethylimidazoleHCID 133631-Chloro-2-(diethylamine)ethane hydrochloride

Product 1

HCID 178464030HCID 178464030, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

4.9 g (60 mmol) of N-methylimidazole are added to 8.6 g (50 mmol) of 2-(diethylamino)ethyl chloride hydrochloride in 50 ml of absolute ethanol and the mixture is refluxed for 12 hours.

Workup

  1. temperaturethe mixture is refluxed for 12 hours

Sources & evidence

ORD record
ord-e291471128d445978400184b03494760
Source dataset
uspto-grants-2000_02
Patent number
US06025496

Reaction notes

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