HCID 54376221, compound → HCID 12392953, compound

Participants

Reaction Steps

This compound was synthesized from 8-(p-methoxyphenyl)-7-octenoic acid (1.24 g, 5 mmol) and Pd/BaSO4 (125 mg) by hydrogenation. Crystallization (petroleum ether) afforded the product (1.20 g, 96%) as white crystals (mp 42-43° C.). IR: 3400-2500, 1705 cm-1 ; 1H-NMR: 1.40 (m, 10H), 2.40 (m, 4H), 3.80 (s, 3H), 6.95 (q, 4H), 10.10 (bs, 1H). Anal. Calcd. for C15H2O2 : C, 71.97, H, 8.86%; Found: C, 72.07, H, 8.88%.

Provenance & Evidence