HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Alcohol → Benzyl 6-Bromohexyl Ether
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Alcohol | HCID 244 | — |
| Reactant | 1,6-Dibromohexane | HCID 12368 | — |
| Product | Benzyl 6-Bromohexyl Ether | HCID 2784764 | 36% |
Reaction Steps
6-Benzyloxyhexyl bromide was prepared from benzyl alcohol (4.75 g, 44 mmol) and 1,6-dibromohexane (9.76 g, 40 mmol) using the general procedure given above. Yield: 36%, bp 100-105° C./torr: 1H-NMR: 1.2-1.9 (m, 8H), 3.37 (t, 4H), 4.46 (s, 2H), 7.28 (m, 5H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06025511 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-528d772813264592abdedb896eb8c876 |
| Source note | uspto-grants-2000_02 |