HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2,4-Dichloro-3-(1'-methoxyimino-1'-(methoxy)methyl)benzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2,4-Dichloro-3-(1'-(methoxy)imino-1'-methoxymethyl)benzoic acid | HCID 53684130 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 2,4-Dichloro-3-(1'-methoxyimino-1'-(methoxy)methyl)benzoyl chloride | HCID 53763003 | 99.8% |
Reaction Steps
A solution of 2.10 g (0.0076 mol) of 2,4-dichloro-3-(1'-(methoxy)imino-1'-methoxymethyl)benzoic acid and 20.00 g of thionyl chloride in 50 ml of dry toluene was stirred for 2 hours at 80° C. After the solvent had been removed in vacuo, 2.25 g of 2,4-dichloro-3-(1'-methoxyimino-1'-(methoxy)methyl)benzoyl chloride were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06028035 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-1b7309e5a5c84657acb3c50eb733269e |
| Source note | uspto-grants-2000_02 |