Isovanillin → HCID 19356269, compound

HRID 377627Notes

Reaction equation

HRID 377627 reaction equation
Br[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1.[OH:21][C:22]1[CH:23]=[C:24]([CH:27]=[CH:28][C:29]=1[O:30][CH3:31])[CH:25]=[O:26]>>[CH3:31][O:30][C:29]1[CH:28]=[CH:27][C:24]([CH:25]=[O:26])=[CH:23][C:22]=1[O:21][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1

Participants

3

Reactant 2

HCID 12127IsovanillinHCID 19356270HCID 19356270, compound

Product 1

HCID 19356269HCID 19356269, compound

Procedure

Reaction of 1-bromo-6-(6-phenylhex-1-yloxy)hexane and 3-hydroxy-4-methoxy benzaldehyde analogous to the procedure of preparation 3, affords the title compound as a pale yellow oil. MS (m/z) 413.

Workup

  1. customto the procedure of preparation 3

Sources & evidence

ORD record
ord-552c8abcab684b2d919a5687834ec43d
Source dataset
uspto-grants-2000_02
Patent number
US06028086

Reaction notes

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