HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 86755158, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 10215486 | HCID 10215486 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86755158 | HCID 86755158 | — |
Reaction Steps
(Z)-5-methoxy-2-methyl-1-(p-methylthiobenzylidene)-3-indenylacetic acid (70 mmol) in absolute THF (500 ml) is heated with oxalylchloride (2 M in CH2Cl2 ; 70 mmol) at reflux (24 hours). The solvent is evaporated to yield the title compound, which is used as such in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06028116 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-6371c52f2ae14383a3885382960eb174 |
| Source note | uspto-grants-2000_02 |