反应详情

A sample of the compound from step 164d (1.2 g, 6.8 mmol) was hydrogenated (4 atm) in ethanol over 1.2 g of 10% Pd/C for 21.5 hours at room temperature. The mixture was filtered to remove the catalyst, and the solvent was removed to afford the title compound (1.055 g). MS m/z (M+H)+ : 151, MS m/z (M+NH4)+ : 168.

1. customfor 21.5 hours
2. customat room temperature
3. filtrationThe mixture was filtered
4. customto remove the catalyst
5. customthe solvent was removed