1-(3,5-Dimethoxyphenyl)piperazine → HCID 54337427, compound

HRID 377848Notes

Reaction equation

HRID 377848 reaction equation
[CH3:1][O:2][C:3]1[C:12]([NH:13][C:14](=[S:16])[O-])=[CH:11][C:10]2[CH2:9][CH2:8][CH2:7][CH2:6][C:5]=2[N:4]=1.[CH3:17][O:18][C:19]1[CH:20]=[C:21]([N:27]2[CH2:32][CH2:31][NH:30][CH2:29][CH2:28]2)[CH:22]=[C:23]([O:25][CH3:26])[CH:24]=1>>[CH3:1][O:2][C:3]1[C:12]([NH:13][C:14]([N:30]2[CH2:29][CH2:28][N:27]([C:21]3[CH:20]=[C:19]([O:18][CH3:17])[CH:24]=[C:23]([O:25][CH3:26])[CH:22]=3)[CH2:32][CH2:31]2)=[S:16])=[CH:11][C:10]2[CH2:9][CH2:8][CH2:7][CH2:6][C:5]=2[N:4]=1

Participants

3

Reactant 2

HCID 27362051-(3,5-Dimethoxyphenyl)piperazineHCID 178493953HCID 178493953, compound

Product 1

HCID 54337427HCID 54337427, compoundYield 56%

Procedure

Phenyl N-[(2-methoxy-5,6,7,8-tetrahydroquinolin-3-yl)thiocarbamate and 1-(3,5-dimethoxyphenyl)piperazine were reacted by the same way with the example 22 to obtain the titled compound.

Sources & evidence

ORD record
ord-42ce7d3c19d34230a53c6f88e5092ff8
Source dataset
uspto-grants-2000_02
Patent number
US06028195

Reaction notes

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