1-(3,5-Dimethoxyphenyl)piperazine → HCID 17893222, compound

HRID 377861Notes

Reaction equation

HRID 377861 reaction equation
[C:1]([C:4]1[CH:5]=[C:6]([NH:13][C:14](=[S:22])OC2C=CC=CC=2)[C:7]([O:11][CH3:12])=[N:8][C:9]=1[CH3:10])(=[O:3])[CH3:2].[CH3:23][O:24][C:25]1[CH:26]=[C:27]([N:33]2[CH2:38][CH2:37][NH:36][CH2:35][CH2:34]2)[CH:28]=[C:29]([O:31][CH3:32])[CH:30]=1>>[C:1]([C:4]1[CH:5]=[C:6]([NH:13][C:14]([N:36]2[CH2:35][CH2:34][N:33]([C:27]3[CH:26]=[C:25]([O:24][CH3:23])[CH:30]=[C:29]([O:31][CH3:32])[CH:28]=3)[CH2:38][CH2:37]2)=[S:22])[C:7]([O:11][CH3:12])=[N:8][C:9]=1[CH3:10])(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 27362051-(3,5-Dimethoxyphenyl)piperazineHCID 54195525HCID 54195525, compound

Product 1

HCID 17893222HCID 17893222, compoundYield 77%

Procedure

Phenyl N-(5-acetyl-2-methoxy-6-methylpyridin-3-yl)thiocarbamate and 1-(3,5-dimethoxyphenyl)piperazine were reacted by the same way with the example 22 to obtain the titled compound.

Sources & evidence

ORD record
ord-f446be19950d45f6b3deeed5a232ad6b
Source dataset
uspto-grants-2000_02
Patent number
US06028195

Reaction notes

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