Phenyl N-(2-methylquinolin-3-yl)carbamate → 1-[(2-Methylquinolin-3-yl)aminocarbonyl]-4-(2-methoxy-5-methylphenyl)piperazine

HRID 377898Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 377898
[CH3:1][C:2]1[C:11]([NH:12][C:13](=[O:21])OC2C=CC=CC=2)=[CH:10][C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[N:3]=1.[CH3:22][O:23][C:24]1[CH:29]=[CH:28][C:27]([CH3:30])=[CH:26][C:25]=1[N:31]1[CH2:36][CH2:35][NH:34][CH2:33][CH2:32]1>>[CH3:1][C:2]1[C:11]([NH:12][C:13]([N:34]2[CH2:33][CH2:32][N:31]([C:25]3[CH:26]=[C:27]([CH3:30])[CH:28]=[CH:29][C:24]=3[O:23][CH3:22])[CH2:36][CH2:35]2)=[O:21])=[CH:10][C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[N:3]=1

Komponenten

3

Edukt 2

HCID 19356949Phenyl N-(2-methylquinolin-3-yl)carbamateHCID 193571151-(2-Methoxy-5-methylphenyl)piperazine

Produkt 1

HCID 193569771-[(2-Methylquinolin-3-yl)aminocarbonyl]-4-(2-methoxy-5-methylphenyl)piperazineAusbeute 80 %

Versuchsvorschrift

Phenyl N-(2-methylquinolin-3-yl)carbamate and 1-(2-methoxy-5-methylphenyl)piperazine were reacted by the same way with the example 114 to obtain the titled compound.

Quellen und Nachweise

ORD-Eintrag
ord-12d4dba459bd4d8ebddbcdfa57926c3f
Quelldatensatz
uspto-grants-2000_02
Patentnummer
US06028195

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