HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → Phenyl N-(4,5-dimethyl-2-methoxyphenyl)carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Phenyl chloroformate | HCID 15891 | — |
| Reactant | 2-Methoxy-4,5-dimethylaniline | HCID 19357140 | — |
| Solvent | Water | HCID 962 | — |
| Product | Phenyl N-(4,5-dimethyl-2-methoxyphenyl)carbamate | HCID 19357180 | 98% |
Reaction Steps
To 4,5-dimethyl-2-methoxyaniline(4.50 g, 0.03 mol), methylene chloride(100 ml) was added and phenyl chloroformate(4.80 g, 0.03 mol) was added slowly. The resulting solution was stirred for 2 hrs and thereto water(150 ml) was added, and extracted with methylene chloride and purified by column chromatography to obtain the titled compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06028195 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-9aaedd679882450eacbdbdc42be67a34 |
| Source note | uspto-grants-2000_02 |