HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorodimethylphenylsilane → n,n-Diethyl-2-chloro-6-(dimethylphenylsilyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorodimethylphenylsilane | HCID 13029 | — |
| Reactant | 2-Chloro-N,N-diethylbenzamide | HCID 82566 | — |
| Product | n,n-Diethyl-2-chloro-6-(dimethylphenylsilyl)benzamide | HCID 54348567 | — |
Reaction Steps
The title compound was prepared from the compound of Example e and 1.1 eq dimethylphenylsilyl chloride according to General Method A. Purification by HPLC with 1:9 ethyl acetate/hexanes gave 6.3 g of the desired product as a clear oil, a 91% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06028101 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-e0368283ae8643caa50546b0ac78faf2 |
| Source note | uspto-grants-2000_02 |