HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 2-Chloro-n-hydroxy-n-(1-methylethyl)-6-(trimethylsilyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | N-Isopropylhydroxylamine Hydrochloride | HCID 170873 | — |
| Reactant | 2-Chloro-6-(trimethylsilyl)benzoyl chloride | HCID 15183557 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 2-Chloro-n-hydroxy-n-(1-methylethyl)-6-(trimethylsilyl)benzamide | HCID 18630150 | — |
Reaction Steps
The title compound was prepared by reaction of the compound of Example b and the i-propylhydroxylamine hydrochloride in dioxane in the presence of two equivalents of triethylamine using the amination methods described above. m.p. 175-179° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06028101 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-f3b2352a9149482ca3a362993dc3a72a |
| Source note | uspto-grants-2000_02 |