HCID 178497929, compound → HCID 178512353, compound

HRID 378117Notes

Reaction equation

HRID 378117 reaction equation
[C:1]([N:3]=[C:4]([NH:13][C:14]1[CH:15]=[C:16]([CH:21]=[CH:22][CH:23]=1)[C:17]([O:19]C)=[O:18])[NH:5]CC1C=CC=CC=1)#[N:2].NC(NC1C=C(C=CC=1)C(OC)=O)=NC#N>>[NH2:5][C:4]([NH:13][C:14]1[CH:15]=[C:16]([CH:21]=[CH:22][CH:23]=1)[C:17]([OH:19])=[O:18])=[N:3][C:1]#[N:2]

Participants

3

Reactant 2

HCID 178497929HCID 178497929, compoundHCID 178497936HCID 178497936, compound

Product 1

HCID 178512353HCID 178512353, compoundYield 92%

Procedure

The title compound was prepared as described in Example I except that the compound of Example E was replaced with an equivalent amount of the compound of Example G. This afforded the title compound (92%) as a white solid.

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-9659f5f2af764021b6fe82a8fc273ee6
Source dataset
uspto-grants-2000_02
Patent number
US06028223

Reaction notes

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