HCID 178464577, compound → HCID 178464576, compound

HRID 378118Notes

Reaction equation

HRID 378118 reaction equation
[C:1]([N:3]=[C:4]([NH:13][C:14]1[CH:15]=[C:16]([CH:21]=[CH:22][CH:23]=1)[C:17]([O:19]C)=[O:18])[NH:5][CH2:6][C:7]1C=CC=CC=1)#[N:2].C(N=C(NC1C=C(C=CC=1)C(OC)=O)NCC)#N>>[C:1]([N:3]=[C:4]([NH:13][C:14]1[CH:15]=[C:16]([CH:21]=[CH:22][CH:23]=1)[C:17]([OH:19])=[O:18])[NH:5][CH2:6][CH3:7])#[N:2]

Participants

3

Reactant 2

HCID 178464577HCID 178464577, compoundHCID 178497929HCID 178497929, compound

Product 1

HCID 178464576HCID 178464576, compoundYield 81%

Procedure

The title compound was prepared as described in Example I except that the compound of Example E was replaced with an equivalent amount of the compound of Example H. This afforded the title compound (81%) as a white solid.

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-c6922c3b46164e498b8f5e80a969643c
Source dataset
uspto-grants-2000_02
Patent number
US06028223

Reaction notes

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