HCID 19353361, compound → HCID 86755176, compound

Participants

Reaction Steps

To a chloroform (3 ml) solution of 9-(1,3-benzodioxol-5-yl)-8-(2-hydroxyethyl)-7-hydroxymethylnaphtho[1,2-d]-1,3-dioxole (36 mg) was added manganese dioxide (360 mg) and stirred for 4 hours, at room temperature. The manganese dioxide was filtered off and the filtrate was concentrated under reduced pressure. The obtained residue was crystallized from ethyl acetate to give the entitled compound (16 mg).

Provenance & Evidence