HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Phenyl-o-phenylenediamine → N-[(3,4,5-trimethoxyphenyl)carbonyl)-N'-phenyl-phenylenediamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Phenyl-o-phenylenediamine | HCID 68297 | — |
| Reactant | Benzoyl chloride, 3,4,5-trimethoxy- | HCID 78282 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | N-[(3,4,5-trimethoxyphenyl)carbonyl)-N'-phenyl-phenylenediamine | HCID 19353961 | — |
Reaction Steps
A solution of N-phenyl-o-phenylenediamine (1.84 g, 10 mmol) in diethyl ether (90 ml) was stirred at room temperature as 3,4,5-trimethoxybenzoyl chloride (2.31 g, 10 mmol) in diethyl ether (40 ml) was added dropwise. The reaction mixture was then stirred overnight at room temperature. The solvents were then removed in vacuo leaving N-[(3,4,5-trimethoxyphenyl)carbonyl]-N'-phenyl-phenylenediamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06030992 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-b606e9ffdc8143ceb1332d8c9fef52a6 |
| Source note | uspto-grants-2000_02 |