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HRID378446

反应详情

EQUATION

反应方程式

HRID 378446 的结构方程式

REACTANTS

反应物

2
结构：OB(O)c1ccc2c(c1)OCO2
HCID2734371

3,4-METHYLENEDIOXYPHENYLBORONIC ACID

C7H7BO4

结构：Cc1cc(NS(=O)(=O)c2ccc(Br)cc2)on1
HCID15453181

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(NS(=O)(=O)c2ccc(-c3ccc4c(c3)OCO4)cc2)on1
HCID15453196

未命名化合物

收率 67%

PROCEDURE

实验过程

N-(3-methyl-5-isoxazolyl)-4-(3,4-methylenedioxyphenyl)benzenesul-fonamide was prepared in the same manner as described in Example 14b, using N-(3-methyl-5-isoxazolyl)-4-bromobenzenesulfonamide and 3,4-methylenedioxyphenylboronic acid resulting in a 67% yield of final product.

WORKUP

后处理

  1. customN-(3-methyl-5-isoxazolyl)-4-(3,4-methylenedioxyphenyl)benzenesul-fonamide was prepared in the same manner