HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Naphthalenesulfonyl chloride → HCID 15453206, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Naphthalenesulfonyl chloride | HCID 66560 | — |
| Reactant | 4-Bromo-5-methyl-1,2-oxazol-3-amine | HCID 2774464 | — |
| Product | HCID 15453206 | HCID 15453206 | 51% |
Reaction Steps
N-(4-Bromo-5-methyl-3-isoxazolyl)-1-naphthalenesulfonamide was prepared from 3-amino-4-bromo-5-methylisoxazole and 1-naphthalenesulfonyl chloride as described in Example 26 in 51% yield. Recrystallization from ethyl acetate/hexanes gave a crystalline solid, m.p. 167-170° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06030991 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-ff3859babcf240c09a53669300fd7a99 |
| Source note | uspto-grants-2000_02 |