HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dichlorobenzene-1-sulfonyl chloride → HCID 18617376, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dichlorobenzene-1-sulfonyl chloride | HCID 2734222 | — |
| Reactant | 4-Bromo-3-methylisoxazol-5-amine | HCID 10487519 | — |
| Product | HCID 18617376 | HCID 18617376 | 75% |
Reaction Steps
2,3-Dichloro-N-(4-bromo-3-methyl-5-isoxazolyl)benzenesulfonamide was prepared from 5-amino-4-bromo-3-methylisoxazole and 2,3-dichlorobenzenesulfonyl chloride according to the procedures described in Example 30. The crude product was purified by recrystallization from ethyl acetate/hexanes to give a crystalline solid, m.p. 166-169° C., yield 75%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06030991 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-2df0f7db00934e868a3472f1db457434 |
| Source note | uspto-grants-2000_02 |