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HRID3785

反应详情

EQUATION

反应方程式

HRID 3785 的结构方程式

REACTANTS

反应物

2
结构：CSCC[C@@H](NC(=O)OC(C)(C)C)C(=O)O
HCID111051

N-(tert-Butyloxycarbonyl)-D-methionine

C10H19NO4S

结构：COC(=O)CN.Cl
HCID122755

Methyl glycinate hydrochloride

C3H8ClNO2

PRODUCTS

生成物

1
结构：COC(=O)CNC(=O)[C@@H](CCSC)NC(=O)OC(C)(C)C
HCID13216971

未命名化合物

PROCEDURE

实验过程

The title compound was prepared by the general method of Example 1 using 24.9 g (0.1 mole) of t-butoxycarbonyl-D-methionine (BOC-D-Met) and 13.8 g (0.11 mole) of glycine methyl ester hydrochloride. The crude product was recrystallized from ethyl acetate/Skellysolve B to give the title compound, which was used in subsequent reactions without further purification.

WORKUP

后处理

  1. customThe crude product was recrystallized from ethyl acetate/Skellysolve B