Toluene → HCID 19353624, compound

HRID 378681Notes

Reaction equation

HRID 378681 reaction equation
[C:1]1([C:24]2[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=2)[CH:6]=[CH:5][C:4]([C:7]2[C:8](=[O:23])[N:9]3[C:14](=[C:15]([C:17]([OH:19])=[O:18])[CH:16]=2)[C:13]2[S:20][CH:21]=[CH:22][C:12]=2[CH:11]=[CH:10]3)=[CH:3][CH:2]=1.O=S(Cl)Cl.[C:34]1(C)C=CC=C[CH:35]=1>C(O)C>[C:1]1([C:24]2[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=2)[CH:2]=[CH:3][C:4]([C:7]2[C:8](=[O:23])[N:9]3[C:14](=[C:15]([C:17]([O:19][CH2:34][CH3:35])=[O:18])[CH:16]=2)[C:13]2[S:20][CH:21]=[CH:22][C:12]=2[CH:11]=[CH:10]3)=[CH:5][CH:6]=1

Participants

5

Reactant 3

HCID 1140TolueneHCID 24386Thionyl ChlorideHCID 19353607HCID 19353607, compound

Product 1

HCID 19353624HCID 19353624, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

From 8-(biphenyl-4-yl)-7-oxo-7H-thieno[2,3-a]quinolizine-10-carboxylic acid with SOCl2 in toluene and ethanol.

Sources & evidence

ORD record
ord-0272f3a158394ec08c2bd3cc8a3ef79e
Source dataset
uspto-grants-2000_02
Patent number
US06030984

Reaction notes

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