HuagongsheHuagongshe Chemistry Print Report · For research reference only
Selectfluor → HCID 21696608, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Selectfluor | HCID 2724933 | — |
| Reactant | HCID 21696638 | HCID 21696638 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 21696608 | HCID 21696608 | — |
Reaction Steps
4-Amino-3-chloro-6-(3,4-dichlorophenoxy)pyridine-2-carboxylic acid was fluorinated with [1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate)] (F-TEDA) in refluxing acetonitrile; mp 156-160° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06297197B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-5285f2cf4db24326aae4b7fbe35a23a9 |
| Source note | uspto-grants-2001_10 |