化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Hydroxide → 2-(Propylthio)pyrimidine-4,6-diol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 1-Iodopropane | HCID 33643 | — |
| 反応物 | HCID 178516656 | HCID 178516656 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 2-(Propylthio)pyrimidine-4,6-diol | HCID 178460810 | — |
反応手順
Propyl iodide (136 ml) was added to a suspension of 4,6-dihydroxy-2-mercaptopyrimidine (200 g) in water (800 ml), containing sodium hydroxide (55.6 g). The reaction mixture was stirred for 2 weeks then concentrated to half volume, 2N hydrochloric acid was added and the subtitle compound was isolated by filtration (167 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06297232B1 |
| 出典データセット | uspto-grants-2001_10 |
| ORD ID | ord-6e83b0f2d6c14146a36cb58912dd272d |
| 出典メモ | uspto-grants-2001_10 |