Nitric Acid → HCID 178460811, compound

HRID 378842Notes

Reaction equation

HRID 378842 reaction equation
[OH:1][C:2]1[CH:7]=[C:6]([OH:8])[N:5]=[C:4]([S:9][CH2:10][CH2:11][CH3:12])[N:3]=1.[N+:13]([O-])([OH:15])=[O:14]>>[OH:1][C:2]1[C:7]([N+:13]([O-:15])=[O:14])=[C:6]([OH:8])[N:5]=[C:4]([S:9][CH2:10][CH2:11][CH3:12])[N:3]=1

Participants

3

Reactant 2

HCID 944Nitric AcidHCID 1784608102-(Propylthio)pyrimidine-4,6-diol

Product 1

HCID 178460811HCID 178460811, compound

Procedure

The product of step (a) (70 g) was added slowly to ice-cooled fuming nitric acid (323 ml). The reaction mixture was stirred for 1 hour then poured onto ice and the subtitle compound was isolated by filtration (65 g).

Workup

  1. additionthen poured onto ice

Sources & evidence

ORD record
ord-5644c745964d4fb581c83b9cd055bf65
Source dataset
uspto-grants-2001_10
Patent number
US06297232B1

Reaction notes

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