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HRID378950

反应详情

EQUATION

反应方程式

HRID 378950 的结构方程式

REACTANTS

反应物

3
结构：CI
HCID6328

Methyl iodide

CH3I

结构：CC(=O)c1cccc(Nc2cc(C)nc(N)n2)c1
HCID133110

Cni H1594

C13H14N4O

结构：CC(=O)c1cccc(Nc2cc(C)[n+](C)c(N)n2)c1
HCID463011

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)c1cccc(Nc2cc(C)[n+](C)c(N)n2)c1.[I-]
HCID12093259

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

Compound No. 14 (CNI-H1494): 4-(3-acetylphenyl)amino-2-amino-6-methylpyrimidine, Compound No. 15, (0.968 g) was suspended in acetone (5 mL) containing methyl iodide (2 mL) was heated at reflux for 48 hr. Filtration after cooling gave 0.657 g of 4-(3-acetylphenyl)amino-2-amino-1,6-dimethylpyrimidinium iodide as a white powder, mp 238-40° C.

WORKUP

后处理

  1. temperaturewas heated
  2. temperatureat reflux for 48 hr
  3. filtrationFiltration
  4. temperatureafter cooling