참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2-Chloroquinoline | HCID 11928 | — |
| 반응물 | Hydrazine hydrate (1:1) | HCID 24654 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Quinoline, 2-hydrazinyl- | HCID 85111 | — |
반응 단계
21.0 g (128.4 mmol) of 2-chloroquinoline are initially charged in 210 ml of ethanol. 64.3 g (1.3 mol) of hydrazine hydrate are added, and the mixture is stirred under reflux for 16 h. The mixture is then cooled to 0° C., and the solid formed is filtered off and washed with a little ethanol. The product is initially air-dried and then dried under high vacuum.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08524699B2 |
|---|
| 출처 데이터셋 | uspto-grants-2013_09 |
|---|
| ORD ID | ord-cfd11d007e1f473c91d1538a8a8ee657 |
|---|
| 출처 메모 | uspto-grants-2013_09 |
|---|
