HuagongsheHuagongshe Chemistry Print Report · For research reference only
THF tetrahydrofurane → DMF dimethylformamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | THF tetrahydrofurane | HCID 22180045 | — |
| Reactant | DME dimethoxyethane | HCID 22508344 | — |
| Reactant | LDA lithium diisopropylamide | HCID 86757460 | — |
| Reactant | HCID 178506870 | HCID 178506870 | — |
| Solvent | Et2O diethylether | HCID 21910879 | — |
| Solvent | DCM Dichloromethane | HCID 21925356 | — |
| Solvent | EtOAc EtOAc | HCID 23514209 | — |
| Product | DMF dimethylformamide | HCID 17824068 | — |
Reaction Steps
THF—tetrahydrofuran; DME—dimethoxyethane; EtOAc—ethyl acetate; Et2O—diethylether; RT—room temperature; LDA—lithium diisopropylamide; CH2Cl2—dichloro-methane; tic—thin layer chromatography; BuLi—butyllithium
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06297264B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-259923fed0f244e6852dbf2247aaf447 |
| Source note | uspto-grants-2001_10 |