化工社化工社 化学情報印刷レポート · 研究参考用
Alpha-Ethyltryptamine → 2-Ethyl 1,2,3,6-tetrahydroazepino[4,5-b]indole-5-carboxylic acid n-propyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Alpha-Ethyltryptamine | HCID 8367 | — |
| 反応物 | Ethyl bromopyruvate | HCID 66144 | — |
| 反応物 | 3-Bromo-2-oxopropionate-1-propyl ester | HCID 11513992 | — |
| 生成物 | 2-Ethyl 1,2,3,6-tetrahydroazepino[4,5-b]indole-5-carboxylic acid n-propyl ester | HCID 66639953 | — |
反応手順
2-Ethyl 1,2,3,6-tetrahydroazepino[4,5-b]indole-5-carboxylic acid n-propyl ester was prepared in a manner similar to that described in Example 1A but replacing tryptamine hydrochloride with α-ethyl tryptamine and ethyl 3-bromopyruvate with n-propyl 3-bromopyruvate; MS (ESI): 303 (MH+).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08524704B2 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-cb2b52eecf044c5b93d30da882410082 |
| 出典メモ | uspto-grants-2013_09 |