1-methyl-1H-1,3-benzodiazole-2-carbaldehyde → HCID 18366587, compound

HRID 379579Notes

Reaction equation

HRID 379579 reaction equation
[CH3:1][N:2]1[C:7](=[O:8])[C:6]2[CH:9]=[CH:10][S:11][C:5]=2[N:4]([CH2:12][CH:13]2[CH2:15][CH2:14]2)[C:3]1=[O:16].[CH3:17][N:18]1[C:22]2[CH:23]=[CH:24][CH:25]=[CH:26][C:21]=2[N:20]=[C:19]1[CH:27]=[O:28]>>[CH:13]1([CH2:12][N:4]2[C:5]3[S:11][C:10]([CH:27]([OH:28])[C:19]4[N:18]([CH3:17])[C:22]5[CH:23]=[CH:24][CH:25]=[CH:26][C:21]=5[N:20]=4)=[CH:9][C:6]=3[C:7](=[O:8])[N:2]([CH3:1])[C:3]2=[O:16])[CH2:14][CH2:15]1

Participants

3

Reactant 2

HCID 7620841-methyl-1H-1,3-benzodiazole-2-carbaldehydeHCID 18366617HCID 18366617, compound

Product 1

HCID 18366587HCID 18366587, compound

Procedure

The title compound was prepared from 3-Methyl-1-(cyclopropylmethyl)thieno[2,3-d]pyrimidine-2,4(1H,3H)-dione (Example 32 step a) and 1-methylbenzimidazole-2-carboxaldehyde following the method of Example 1 step d.

Sources & evidence

ORD record
ord-405c4dbcc62342c884f8326637fe2fba
Source dataset
uspto-grants-2001_10
Patent number
US06300334B1

Reaction notes

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