Ethanol → HCID 9884881, compound

HRID 379697Notes

Reaction equation

HRID 379697 reaction equation
[NH2:1][CH2:2][CH2:3][O:4][C:5]1[CH:23]=[CH:22][C:8]([NH:9][C:10](=[O:21])[C:11]2[C:16]([O:17][CH3:18])=[CH:15][CH:14]=[CH:13][C:12]=2[O:19][CH3:20])=[CH:7][CH:6]=1.C(O)C.[ClH:27].C(O)C>C(OCC)C>[ClH:27].[NH2:1][CH2:2][CH2:3][O:4][C:5]1[CH:23]=[CH:22][C:8]([NH:9][C:10](=[O:21])[C:11]2[C:12]([O:19][CH3:20])=[CH:13][CH:14]=[CH:15][C:16]=2[O:17][CH3:18])=[CH:7][CH:6]=1

Participants

5

Reactant 3

HCID 702EthanolHCID 9884882HCID 9884882, compoundHCID 21887872Ethanol hydrochloride

Product 1

HCID 9884881HCID 9884881, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

4′-(2-Aminoethoxy)-2,6-dimethoxybenzanilide (0.74 g) was dissolved into ethanol (5 ml) and added with 1N HCl/ethanol (5 ml). The solution was added with diethyl ether (100 ml). The precipitate was collected and dried under vacuum to obtain 4′-(2-aminoethoxy)-2,6-dimethoxybenzanilide hydrochloride (0.73 g) as white powder.

Workup

  1. customThe precipitate was collected
  2. customdried under vacuum

Sources & evidence

ORD record
ord-05f6dd464c834b919fb0140f35dc6403
Source dataset
uspto-grants-2001_10
Patent number
US06300368B1

Reaction notes

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