HCID 18367729, compound → HCID 18367767, compound

HRID 379726Notes

Reaction equation

HRID 379726 reaction equation
[C:1]([NH:4][C:5]1[C:13]2[C:8](=[CH:9][C:10]([Cl:14])=[CH:11][CH:12]=2)[N:7](C(OCC)=O)[C:6]=1[C:20](=[O:29])[C:21]1[CH:26]=[CH:25][C:24]([O:27][CH3:28])=[CH:23][CH:22]=1)(=[O:3])[CH3:2]>C(O)C.CCCCCC>[C:1]([NH:4][C:5]1[C:13]2[C:8](=[CH:9][C:10]([Cl:14])=[CH:11][CH:12]=2)[NH:7][C:6]=1[C:20](=[O:29])[C:21]1[CH:26]=[CH:25][C:24]([O:27][CH3:28])=[CH:23][CH:22]=1)(=[O:3])[CH3:2]

Participants

3

Reactant 1

HCID 18367729HCID 18367729, compound

Product 1

HCID 18367767HCID 18367767, compound

Reagents, catalysts & solvents 1

HCID 21879635Ethanol hexaneSolvent

Procedure

The title compound was prepared according to the procedure described in step 2 of Example 2 (Method A) from 3-acetylamino-6-chloro-1-ethoxycarbonyl-2-(4-methoxybenzoyl)indole (step 2). m.p.: 137-139° C. (ethanol/hexane)

Sources & evidence

ORD record
ord-4f27c8429c47409d87bc039b350ee713
Source dataset
uspto-grants-2001_10
Patent number
US06300363B1

Reaction notes

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