huagongshe.com
HRID379739

反应详情

EQUATION

反应方程式

HRID 379739 的结构方程式

REACTANTS

反应物

2
结构：CCC(=O)Cl
HCID62324

Propanoyl chloride

C3H5ClO

结构：Nc1c(C(=O)c2cccc(Cl)c2)[nH]c2cc(Cl)ccc12
HCID18368029

未命名化合物

PRODUCTS

生成物

1
结构：CCC(=O)Nc1c(C(=O)c2cccc(Cl)c2)[nH]c2cc(Cl)ccc12
HCID18367965

未命名化合物

PROCEDURE

实验过程

The title compound was prepared according to the procedure described in Example 19 employing 3-amino-6-chloro-2-(3-chlorobenzoyl)indole (Example 30) and propionyl chloride. m.p.: 129-130° C. 1H-NMR (CDCl3): 9.95 (1H, br s), 8.30 (1H, d, J=9.2 Hz), 8.17 (1H, br s), 7.78-7.59 (3H, m), 7.51 (1H, t, J=7.7 Hz), 7.32 (1H, d, J=1.1 Hz), 7.11 (1H, dd, J=1.8, 8.8 Hz), 4.48 (2H, q, J=7.6 Hz), 1.30 (3H, t, J=7.6 Hz)