Acetyl chloride → HCID 18367885, compound

HRID 379774Notes

Reaction equation

HRID 379774 reaction equation
[NH2:1][C:2]1[C:10]2[C:5](=[CH:6][C:7]([Cl:11])=[CH:8][CH:9]=2)[NH:4][C:3]=1[C:12]([C:14]1[CH:18]=[CH:17][O:16][CH:15]=1)=[O:13].[C:19](Cl)(=[O:21])[CH3:20]>C(OCC)(=O)C.CCCCCC>[C:19]([NH:1][C:2]1[C:10]2[C:5](=[CH:6][C:7]([Cl:11])=[CH:8][CH:9]=2)[NH:4][C:3]=1[C:12]([C:14]1[CH:18]=[CH:17][O:16][CH:15]=1)=[O:13])(=[O:21])[CH3:20]

Participants

4

Reactant 2

HCID 6367Acetyl chlorideHCID 18368076HCID 18368076, compound

Product 1

HCID 18367885HCID 18367885, compound

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

The title compound was prepared according to the procedure described in Example 19 from 3-amino-6-chloro-2-(3-furoyl)indole (Example 79) and acetyl chloride. m.p.:217-219° C. (ethyl acetate/hexane)

Sources & evidence

ORD record
ord-705c84af893e4962a0dc2bc259683583
Source dataset
uspto-grants-2001_10
Patent number
US06300363B1

Reaction notes

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