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HRID 37980作成日：2026年10月25日

4-Methyl-3-nitrobenzenesulfonyl chloride → 3-(4-Methyl-3-nitrobenzenesulfonyl)-1,2,3,6-tetrahydroazepino[4,5-B]indole-5-carboxylic acid ethyl ester

https://huagongshe.com/reaction/37980

反応式

関与物質

役割名称HCID仕込み量
反応物4-Methyl-3-nitrobenzenesulfonyl chlorideHCID 560638—
反応物Ethyl 1,2,3,6-tetrahydroazepino[4,5-B]indole-5-carboxylateHCID 57467979—
生成物3-(4-Methyl-3-nitrobenzenesulfonyl)-1,2,3,6-tetrahydroazepino[4,5-B]indole-5-carboxylic acid ethyl esterHCID 57559157—

反応手順

The title compound was prepared in a manner similar to that described in Example 70 by using ethyl-1,2,3,6-tetrahydroazepino[4,5-b]indole-5-carboxylate and 4-methyl-3-nitrobenzenesulfonyl chloride (˜3.4 mg); MS (ES): 456 (MH+).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US08524704B2
出典データセットuspto-grants-2013_09
ORD IDord-d4cd283f793a4b0da4b156c89f149435
出典メモuspto-grants-2013_09