Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Amino-6-chlorobenzonitrile → Ethyl (3-chloro-2-cyanophenyl)carbamate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Amino-6-chlorobenzonitrile | HCID 81056 | — |
| 반응물 | Ethyl acetate hexane | HCID 21226206 | — |
| 생성물 | Ethyl (3-chloro-2-cyanophenyl)carbamate | HCID 15048424 | — |
반응 단계
The title compound was prepared according to the procedure described in step 1 of Example 1 (Method B) from 2-amino-6-chlorobenzonitrile. m.p.: 144.5-145.1 (ethyl acetate/hexane) 1H-NMR (CDCl3) δ: 8.21 (1H, d, J=8 Hz), 7.49 (1H, t, J=8 Hz), 7.16 (1H, d, J=8 Hz), 7.17 (1H, br s), 4.27 (2H, q, J=7 Hz), 1.35 (3H, t, J=7 Hz)
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06300363B1 |
| 출처 데이터셋 | uspto-grants-2001_10 |
| ORD ID | ord-3336286e8cb94447a136f2764638378f |
| 출처 메모 | uspto-grants-2001_10 |