HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenacyl bromide → 3-Amino-2-benzoyl-4-chloro-1-(ethoxycarbonyl)indole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenacyl bromide | HCID 6259 | — |
| Reactant | Diisopropyl Ether | HCID 7914 | — |
| Reactant | Ethyl (3-chloro-2-cyanophenyl)carbamate | HCID 15048424 | — |
| Product | 3-Amino-2-benzoyl-4-chloro-1-(ethoxycarbonyl)indole | HCID 18367913 | — |
Reaction Steps
The title compound was prepared according to the procedure described in step 2 of Example 1 from 6-chloro-2-(ethoxycarbonylamino)benzonitrile (step 1) and 2-bromoacetophenone. m.p.: 118-119° C. (isopropyl ether)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06300363B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-461e5f61cbdb4699a722e96c229cba6a |
| Source note | uspto-grants-2001_10 |