HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl bromoacetate → HCID 53981456, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl bromoacetate | HCID 60984 | — |
| Reactant | 4-Chloro-2-[(ethoxycarbonyl)amino]benzonitrile | HCID 18367888 | — |
| Product | HCID 53981456 | HCID 53981456 | — |
Reaction Steps
The title compound was prepared according to the procedure described in step 2 of Example 1 from 4-chloro-2-(ethoxycarbonylamino)benzonitrile (Example 1, step 2) and methyl bromoacetate. 1H-NMR (CDCl3) δ: 8.08 (1H, d, J=1.8 Hz), 7.42 (1H, d, J=8.8 Hz), 7.22 (1H, dd, J=8.8, 1.8 Hz), 5.17 (2H, br s), 4.40 (2H, q, J=7.3 Hz), 3.88 (3H, s), 1.40 (3H, t, J=7.3 Hz)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06300363B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-458f00a63b034a5d8137670d84e1fd42 |
| Source note | uspto-grants-2001_10 |