3-[3-Amino-6-chloro-1-(ethoxycarbonyl)indole-2-carbonyl]benzenesulfonamide → 3-(3-Amino-6-chloroindole-2-carbonyl)benzenesulfonamide
Reaction equation
[NH2:1][C:2]1[C:10]2[C:5](=[CH:6][C:7]([Cl:11])=[CH:8][CH:9]=2)[N:4](C(OCC)=O)[C:3]=1[C:17]([C:19]1[CH:20]=[C:21]([S:25]([NH2:28])(=[O:27])=[O:26])[CH:22]=[CH:23][CH:24]=1)=[O:18]>CC(O)C.C1(C)C=CC=CC=1>[NH2:1][C:2]1[C:10]2[C:5](=[CH:6][C:7]([Cl:11])=[CH:8][CH:9]=2)[NH:4][C:3]=1[C:17]([C:19]1[CH:20]=[C:21]([S:25]([NH2:28])(=[O:26])=[O:27])[CH:22]=[CH:23][CH:24]=1)=[O:18]Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
The title compound was prepared according to the procedure described in step 2 of Example 1 employing 3-[3-amino-6-chloro-1-(ethoxycarbonyl)indole-2-carbonyl]benzenesulfonamide (step 1). m.p.: 125-127° C. (2-propanol/toluene)
Sources & evidence
- ORD record
- ord-e246fd5d0c5a446a844aaf305ad769b7
- Source dataset
- uspto-grants-2001_10
- Patent number
- US06300363B1
Reaction notes
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