HCID 18367959, compound → HCID 18368093, compound

HRID 379846Notes

Reaction equation

HRID 379846 reaction equation
[NH2:1][C:2]1[C:10]2[C:5](=[CH:6][C:7]([Cl:11])=[CH:8][CH:9]=2)[N:4](C(OCC)=O)[C:3]=1[C:17]([CH:19]1[CH2:24][CH2:23][CH2:22][CH:21]([CH3:25])[CH2:20]1)=[O:18]>CCCCCC.C(OCC)(=O)C>[NH2:1][C:2]1[C:10]2[C:5](=[CH:6][C:7]([Cl:11])=[CH:8][CH:9]=2)[NH:4][C:3]=1[C:17]([CH:19]1[CH2:24][CH2:23][CH2:22][CH:21]([CH3:25])[CH2:20]1)=[O:18]

Participants

3

Reactant 1

HCID 18367959HCID 18367959, compound

Product 1

HCID 18368093HCID 18368093, compound

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

The title compound was prepared according to the procedure described in step 3 of Example 1 from 3-amino-6-chloro-1-ethoxycarbonyl-2-(3-methylcyclohexylcarbonyl)indole (step 2). m.p.: 140-142° C. (hexane/ethyl acetate)

Sources & evidence

ORD record
ord-39c1e993c38846e8b3e1104112d3e8c1
Source dataset
uspto-grants-2001_10
Patent number
US06300363B1

Reaction notes

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