HCID 18367755, compound → HCID 18367957, compound
Reaction equation
[C:1]([NH:4][C:5]1[C:13]2[C:8](=[CH:9][C:10]([Cl:14])=[CH:11][CH:12]=2)[N:7](C(OCC)=O)[C:6]=1[C:20](=[O:28])[C:21]1[CH:26]=[CH:25][CH:24]=[C:23]([CH3:27])[CH:22]=1)(=[O:3])[CH3:2].[CH2:29](O)C.C(OCC)C>>[C:1]([N:4]([C:5]1[C:13]2[C:8](=[CH:9][C:10]([Cl:14])=[CH:11][CH:12]=2)[NH:7][C:6]=1[C:20](=[O:28])[C:21]1[CH:26]=[CH:25][CH:24]=[C:23]([CH3:27])[CH:22]=1)[CH3:29])(=[O:3])[CH3:2]Participants
3
Procedure
The title compound was prepared from 3-acetylamino-6-chloro-1-ethoxycarbonyl-2-(3-methylbenzoyl)indole (Example 22, step 1) according to the procedure described in Example 146. m.p.: 166-171° C. (ethanol/diethyl ether)
Sources & evidence
- ORD record
- ord-0f327e37419b46539a542107c7548fbc
- Source dataset
- uspto-grants-2001_10
- Patent number
- US06300363B1
Reaction notes
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