HCID 18367768, compound → HCID 18367742, compound

HRID 379851Notes

Reaction equation

HRID 379851 reaction equation
[C:1]([NH:4][C:5]1[C:13]2[C:8](=[CH:9][C:10]([Cl:14])=[CH:11][CH:12]=2)[N:7](C(OCC)=O)[C:6]=1[C:20]([CH:22]1[CH2:27][CH2:26][CH2:25][CH2:24][CH2:23]1)=[O:21])(=O)C.[C:28](OCC)(=[O:30])[CH3:29].CCCCCC>>[C:28]([N:4]([C:5]1[C:13]2[C:8](=[CH:9][C:10]([Cl:14])=[CH:11][CH:12]=2)[NH:7][C:6]=1[C:20]([CH:22]1[CH2:27][CH2:26][CH2:25][CH2:24][CH2:23]1)=[O:21])[CH3:1])(=[O:30])[CH3:29]

Participants

3

Reactant 2

HCID 18367768HCID 18367768, compoundHCID 21226206Ethyl acetate hexane

Product 1

HCID 18367742HCID 18367742, compound

Procedure

The title compound was prepared from 3-acetylamino-6-chloro-2-cyclohexylcarbonyl-1-(ethoxycarbonyl)indole (step 1) according to the procedure described in Example 146. m.p.: 162-163° C. (ethyl acetate/hexane)

Sources & evidence

ORD record
ord-272924f3ee8d454e80c335e32b798eb7
Source dataset
uspto-grants-2001_10
Patent number
US06300363B1

Reaction notes

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