HCID 18367875, compound → HCID 18367933, compound

HRID 379854Notes

Reaction equation

HRID 379854 reaction equation
[C:1]([C:9]1[N:10](C(OCC)=O)[C:11]2[C:16]([C:17]=1[N:18]([CH3:20])[CH3:19])=[CH:15][CH:14]=[C:13]([Cl:21])[CH:12]=2)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1>C(OCC)C.CCCCCC>[C:1]([C:9]1[NH:10][C:11]2[C:16]([C:17]=1[N:18]([CH3:19])[CH3:20])=[CH:15][CH:14]=[C:13]([Cl:21])[CH:12]=2)(=[O:8])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 1

HCID 18367875HCID 18367875, compound

Product 1

HCID 18367933HCID 18367933, compound

Reagents, catalysts & solvents 1

HCID 21584099Diethylether hexaneSolvent

Procedure

The title compound was prepared according to the procedure described in step 2 of Example 2 from 2-benzoyl-6-chloro-1-ethoxycarbonyl-3-(N,N-dimethylamino)indole (step 1). m.p.: 178-180° C. (diethyl ether/hexane)

Sources & evidence

ORD record
ord-ca027214bb804d2b8570e35d98bc8adb
Source dataset
uspto-grants-2001_10
Patent number
US06300363B1

Reaction notes

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