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HRID379867

反应详情

EQUATION

反应方程式

HRID 379867 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)OC(C)(C)C(=O)Cl
HCID123496

2-Acetoxyisobutyroyl chloride

C6H9ClO3

结构：Nc1c(C(=O)c2cc(Cl)ccn2)[nH]c2cc(Cl)ccc12
HCID18368126

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)OC(C)(C)C(=O)Nc1c(C(=O)c2cc(Cl)ccn2)[nH]c2cc(Cl)ccc12
HCID18368167

未命名化合物

PROCEDURE

实验过程

The title compound was prepared according to the procedure described in Example 19 employing 3-amino-6-chloro-2-(4-chloropyridine-2-carbonyl)indole (Exampe 68) and 2-acetoxyisobutyryl chloride. m.p.: 228-229° C. (recrystallized from ethyl acetate) IR(KBr)ν: 3500, 3250, 1740, 1710, 1620, 1600, 1570, 1540, 1480, 1350, 1230, 1180, 1150, 740 cm−1.