HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Bromobenzenesulphonyl chloride → HCID 18367534, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Bromobenzenesulphonyl chloride | HCID 17943 | — |
| Reactant | N,N-Dimethylethylenediamine | HCID 66053 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 18367534 | HCID 18367534 | 62.8% |
Reaction Steps
N,N-Dimethylethylenediamine (1.76 g) was added dropwise to a solution of 3-bromobenzenesulfonyl chloride (5.11 g) in diethyl ether (100 ml) at room temperature. The resulting suspension was stirred for 30 minutes and filtered to afford the sub-title compound as a solid (4.31 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06300352B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-557360cc46524f7a8315e7120e408139 |
| Source note | uspto-grants-2001_10 |