참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Oxygen | HCID 977 | — |
| 반응물 | Hexanal, 6-hydroxy- | HCID 190319 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 6-Hydroxyhexanoic Acid | HCID 14490 | — |
반응 단계
5.28 Grams (45 mmols) of 6-hydroxyhexanal was charged to a 100 milliliter Schlenk flask and dissolved in 45 milliliters of deionized water by heating to 85-95° C. in a water bath. The resulting solution was charged to the Parr autoclave, placed under 1500 psi O2 and heated to 120° C. Samples were taken every 30 minutes throughout the reaction. After 1.5 hours, reaction conversion was 92% and 6-hydroxycaproic acid was formed in 92% selectivity.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06300496B1 |
|---|
| 출처 데이터셋 | uspto-grants-2001_10 |
|---|
| ORD ID | ord-02d90ac0134c4de78ab92718b4fc89cc |
|---|
| 출처 메모 | uspto-grants-2001_10 |
|---|
