HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-[Hydroxy(3-methoxyphenyl)methyl)-2-oxotetrahydrofuran → 3-(3-Methoxybenzyl)-2-oxotetrahydrofuran
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-[Hydroxy(3-methoxyphenyl)methyl)-2-oxotetrahydrofuran | HCID 18367294 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-(3-Methoxybenzyl)-2-oxotetrahydrofuran | HCID 18367364 | 86.2% |
Reaction Steps
A mixture of 3-[hydroxy(3-methoxyphenyl)methyl]-2-oxotetrahydrofuran (1.0 g) and 10% Pd/C (0.5 g) in ethanol (20 ml) was stirred under H2 for 10 hours. The catalyst was filtered off and the filtrate was evaporated in vacuo to give 3-(3-methoxybenzyl)-2-oxotetrahydrofuran (0.8 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06300344B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-e4a510a9640f4e029356e7f2dd1100ff |
| Source note | uspto-grants-2001_10 |